Titlebook: Chiral Separations; D. Stevenson,I. D. Wilson Book 1988 Springer Science+Business Media New York 1988 alcohol.amino acid.chemistry.chromat

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, the Role of Solvents and Steric Factors in the Resolution of β-Blocker Drugs on Chiral Urea Phases has been known for sometime[1] that the L form shows a 50 to 500 fold greater activity than the D form. Furthermore the work of Nelson and Burke[2] demonstrated that some of the metabolites of the D form showed signs of toxicity. In view of these findings, there has been a natural interest in the resolution of these drugs and their metabolities.

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Use of Various Commercially Available Chiral Stationary Phases in Supercritical Fluid ChromatograpAt the same time, there has been much interest in the field of chiral separations[4], exemplified by the development of many chiral stationary phases (CSPs), many of which are now commercially available.

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Strategies for Optimising Chiral Separations in Drug Analysis,of the enantiomers of oxamniquine on a first-generation α.-acid glycoprotein phase. The performance of these approaches is discussed, and the potential contribution of novel chiral detector technology is considered with reference to more fully automated optimisation schemes in chiral HPLC.

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Prospects for Chiral Thin-Layer Chromatography,) for TLC of wide general applicability is noted and contrasted with advances in chiral methodology for high performance liquid and gas liquid chromatography. The need for further research into the preparation of CSP s, to enable enantioselective separations to be performed on TLC is highlighted and recent progress towards this goal described.

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Separation of Enantiomers of Oxyphenonium Bromide by High-Performance Liquid Chromatography,iomers of this drug exhibit large differences in therapeutic effects as well as in biliary and urinary excretion[1]. For a detailed study of the fate of oxyphenonium bromide enantiomers in the body, an assay is required that allows the simultaneous determination of the two enantiomers in the same sa

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