书目名称 | Quantitative EPR | 编辑 | Gareth R. Eaton,Sandra S. Eaton,Ralph T. Weber | 视频video | | 概述 | Practical guide for people who perform EPR measurements, or supervise the use of EPR spectroscopy.No existing book provides this level of practical guidance to ensure successful use of EPR.Careful att | 图书封面 |  | 描述 | There is a growing need in both industrial and academic research to obtain accurate quantitative results from continuous wave (CW) electron paramagnetic resonance (EPR) experiments. This book describes various sample-related, instrument-related and software-related aspects of obtaining quantitative results from EPR expe- ments. Some speci?c items to be discussed include: selection of a reference standard, resonator considerations (Q, B ,B ), power saturation, sample position- 1 m ing, and ?nally, the blending of all the factors together to provide a calculation model for obtaining an accurate spin concentration of a sample. This book might, at ?rst glance, appear to be a step back from some of the more advanced pulsed methods discussed in recent EPR texts, but actually quantitative “routine CW EPR” is a challenging technique, and requires a thorough understa- ing of the spectrometer and the spin system. Quantitation of CW EPR can be subdivided into two main categories: (1) intensity and (2) magnetic ?eld/mic- wave frequency measurement. Intensity is important for spin counting. Both re- tive intensity quantitation of EPR samples and their absolute spin concentration of samples are | 出版日期 | Book 2010 | 关键词 | EPR; Quantitative EPR; calibration; distribution; hyperfine splitting; spectra; spectroscopy; spin; temperat | 版次 | 1 | doi | https://doi.org/10.1007/978-3-211-92948-3 | isbn_softcover | 978-3-7091-1681-4 | isbn_ebook | 978-3-211-92948-3 | copyright | Springer-Verlag Vienna 2010 |
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