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Titlebook: Dynamical Decoupling in Distance Measurements by Double Electron-Electron Resonance; Janne Marie Soetbeer Book 2016 The Editor(s) (if appl

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https://doi.org/10.1007/978-3-662-08690-2n electron spin pairs introduced in biomolecules by site-directed spin labelling (SDSL) in the nanometer range. The obtainable distance range and sensitivity of the DEER experiment strongly depends on the transverse relaxation of the electron spin as this determines the maximal available dipolar evolution time in the DEER experiment.
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Introduction and Theory,n electron spin pairs introduced in biomolecules by site-directed spin labelling (SDSL) in the nanometer range. The obtainable distance range and sensitivity of the DEER experiment strongly depends on the transverse relaxation of the electron spin as this determines the maximal available dipolar evolution time in the DEER experiment.
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https://doi.org/10.1007/978-3-662-08690-2n electron spin pairs introduced in biomolecules by site-directed spin labelling (SDSL) in the nanometer range. The obtainable distance range and sensitivity of the DEER experiment strongly depends on the transverse relaxation of the electron spin as this determines the maximal available dipolar evo
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Janne Marie SoetbeerStudy in Natural Science.Includes supplementary material:
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978-3-658-14669-6The Editor(s) (if applicable) and The Author(s), under exclusive license to Springer Fachmedien Wies
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https://doi.org/10.1007/978-3-662-08690-2Model systems were chosen to mimic typical DEER application scenarios for which the relaxation behaviour of the nitroxide spin in the different spin environments (i.e. protonated, partly or completely deuterated solvent) was studied.
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https://doi.org/10.1007/978-3-662-08690-2Relaxation measurements for all samples were carried out. The resulting relaxation traces for TEMPOL, T4 Lysozyme, WALP23 and MS107 at Q-band frequencies were normalised by the maximum signal intensity of the 4-DEER trace. This normalisation allows to compare the refocusing scheme performance relative to the 4-DEER setup as a function of time.
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