Withdrawal 发表于 2025-3-21 20:07:57

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dagger 发表于 2025-3-21 21:01:36

5-Bromo-2-Furoic Acid,o absorb hydrogen bromide liberated in the reaction, the top of the condenser was connected to a Tishchenko vessel containing a solution of alkali. A mixture of 112 g (1 mole) of 2-furoic acid (see p. 43), m.p. 128–132°, 10 g of dry red phosphorus, and 800 ml of chloroform was prepared in the flask.

创作 发表于 2025-3-22 02:57:14

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anthesis 发表于 2025-3-22 08:19:17

5-(Diethylaminomethyl) Furfuryl Alcohol,ise over a period of 0.5–1 hour to a stirred ethereal solution (200 ml) of lithium aluminum hydride (Note 1) contained in a 500-ml three-necked flask fitted with mercury-sealed stirrer, dropping funnel, and reflux condenser protected by a calcium chloride tube.

原谅 发表于 2025-3-22 09:50:33

Methyl 5-Benzyl-2-Furoate,-ml three-necked round-bottomed flask fitted with mercury-sealed stirrer and reflux condenser protected by a calcium chloride tube, and it was stirred and cooled with ice water for two hours while 40 g (0.3 mole) of anhydrous aluminum chloride was added in small portions. When the vigorous reaction

顽固 发表于 2025-3-22 15:19:09

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提升 发表于 2025-3-22 17:38:41

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冥界三河 发表于 2025-3-22 23:14:45

Methyl 5-(Diethylaminomethyl)-2-Furoate,l round-bottomed flask fitted with reflux condenser and dropping funnel. The solution was cooled with ice water, and a solution of 14.6 g (0.2 mole) of diethylamine in 30 ml of dry benzene was added over a period of ten minutes.

BORE 发表于 2025-3-23 02:35:22

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无脊椎 发表于 2025-3-23 08:46:40

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查看完整版本: Titlebook: Synthesis of Heterocyclic Compounds; A. L. Mndzhoian Book 1959 Springer-Verlag US 1959 Alkaloid.alkaloids.biology.chemistry.cyclic compoun